Interlaboratory testing for the determination of trace amounts of tin and lead in magnesium and magnesium alloys by inductively coupled plasma atomic emission spectrometry.

نویسندگان

  • Michihisa Uemoto
  • Makoto Nagaoka
  • Hiroshi Fujinuma
چکیده

In order to establish a standard analytical method for the determination of trace amounts of tin and lead in magnesium and its alloys, which could be found in neither JIS nor ISO standards, an interlaboratory testing with inductively coupled plasma atomic emission spectrometry (ICP-AES) has been put into practice. Simple dissolution with nitric and hydrochloric acids and sample nebulization procedures were finally concluded to be suitable for standardization. The analytical methods, proposed in this study have been provided as newly established JIS standards.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Selective Separation and Preconcentration of trace Amounts of Gallium in Water and Rice Samples using Cloud Point Extraction and Determination by Inductively Coupled Plasma-Atomic Emission Spectrometry

In the present study a cloud-point extraction process using non-ionic surfactant Triton X-114 for selective extraction of gallium from aqueous solutions was developed. The method is based on the complex formation of Ga (III) with N, N′ -bis (salycilidene)-1, 2-phenylenediamine (salophen) as a chelating agent in buffer media of pH 5. After phase separation and dilution of the surfactant-rich pha...

متن کامل

Screening and Optimization of Microextraction of Pb(II) by Inductively Coupled Plasma-Atomic Emission Using Response Surface Methodology

Dispersive liquid–liquid microextraction (DLLME) combined with inductively coupled plasma-atomic emission spectrometry (ICP-AES) was applied for the determination of lead in different environmental water samples. Ammonium pyrrolidine dithiocarbamate (APDC), chloroform and ethanol were used as chelating agent, extraction solvent and disperser solvent, respectively. The effective parameters, such...

متن کامل

Review of preconcentration and solid phase extraction for the determination of trace Lead

Spectrometric techniques for the analysis of trace lead have developed rapidly due to the increasing need for accurate measurements at extremely low levels of this element in diverse matrices. This review covers separation and preconcentration procedures, and considers the features of the application with several spectrometric techniques. The use of an appropriate sample handling technique is a...

متن کامل

Review of preconcentration and solid phase extraction for the determination of trace Lead

Spectrometric techniques for the analysis of trace lead have developed rapidly due to the increasing need for accurate measurements at extremely low levels of this element in diverse matrices. This review covers separation and preconcentration procedures, and considers the features of the application with several spectrometric techniques. The use of an appropriate sample handling technique is a...

متن کامل

Determination of 137Ba Isotope Abundances in Water Samples by Inductively Coupled Plasma-optical Emission Spectrometry Combined with Least-squares Support Vector Machine Regression

A simple and rapid method for the determination of 137Ba isotope abundances in water samples by inductively coupled plasma-optical emission spectrometry (ICP-OES) coupled with least-squares support vector machine regression (LS-SVM) is reported. By evaluation of emission lines of barium, it was found that the emission line at 493.408 nm provides the best results for the determination...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Analytical sciences : the international journal of the Japan Society for Analytical Chemistry

دوره 25 5  شماره 

صفحات  -

تاریخ انتشار 2009